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WAT-70Xi: Wax Appearance Temperature

A Breakthrough in Crude Oil and Marine Fuel Oil Testing

State-of-the-Art Solution

Phase Technology’s WAT-70Xi analyzer is the world’s first and only fully automatic instrument to measure Wax Appearance Temperature (WAT) and Wax Disappearance Temperature (WDT) of crude and marine fuel oils, capable of performing reliable testing of VLSFO and residual black oils.

Product Overview

With a long, notable history as the world leader in developing test methods for cold flow properties detection, Phase Technology has now extended its capability to include a critical measurement for crude oil: Wax Appearance Temperature (WAT).

Also known as cloud point, wax appearance temperature is the temperature at which a crude oil sample first precipitates solid wax as it is being cooled under prescribed test conditions.

Similarly, Wax Disappearance Temperature (WDT) is the temperature at which the last wax solids are melted into liquid during a warming cycle.

Until now, trying to determine crude oil WAT or cloud point was an imprecise, tedious, and subjective process. Various manual methods have been tried, but all are difficult and timeconsuming, yielding results with unacceptably wide error margins.

Phase Technology’s WAT-70Xi analyzer revolutionizes the upstream, midstream oil and marine fuel industries with the world’s first and only fully automatic process to measure WAT and WDT of crude and marine fuel oils. Following ASTM D8420 method, our proprietary optical light scattering technique detects phase changes with extreme sensitivity and accuracy.

This important scientific break-through means that even the darkest, most opaque samples can now be easily tested, with 1.0° C precision. The Phase Technology WAT-70Xi offers a considerable efficiency advantage—just load the sample, and the analyzer does the rest, with tests completed in just 20-40 minutes. There’s no time-consuming manual set-up needed, and cleaning is done automatically after each test.

Benefits:

  • Detection of both WAT and WDT – two critical tests for understanding crude and marine fuel oil behavior.
  • Faster than any other test method – results in just 20-40 minutes, compared to average test times of several hours for other methods.
  • Tests opaque samples – enhanced optical configuration “sees” through dark samples.
  • Self cleaning – automatic solvent flush after each test run.
  • No manual set up – simply inject sample directly into analyzer and being test run.
  • Superior precision – repeatability of 1.0°C
  • Greater sensitivity – controlled, automatic test method ensures no subjectivity in reported results.
  • Informative, real-time test results – complete phase diagram (loop) clearly illustrates WAT, relative amount of wax formation and WDT.

Key Features

1

Critical testing for understanding crude and marine fuel oil behavior.

2

Faster than any other test method – results in just 20-40 minutes

3

Tests opaque samples.

4

Automatic self cleaning after each test run.

5

No manual set up

6

Superior precision – repeatability of 1.0°C

7

Greater sensitivity to ensure no subjectivity in results.

8

Informative, real-time test results

9

Easy-to-use touch interface

Specs

Test Methods & Precision

Test Method: ASTM D8420 Standard test method for wax appearance temperature and wax disappearance temperature of petroleum products and liquid fuels

Repeatability: 1.0°C

Operation

Detection: Diffusive Light Scattering (DLS) technology

Cooling System: Integrated Peltier device cooling system Linear cooling profiles according to method

System Cleaning: Automatic solvent flush cycle

Application Range

Temperature Range:
Sample: -30 to +65°C °C or °F (user selectable)
Test Resolution: 0.1°C

Measurements

Sample Size: 3.0 mL

Test Duration: 20 to 40 minutes

Required Operator Time: 0.25 minutes

Documentation

Printing Label printer: Detailed test report in °C or °F with date & time stamped, sample information, test mode

Full-size printer: Detailed detection curve tracking of fuel behaviors during the test; can be printed as part of test report.

Internal Memory: Storage up to 5000 test runs

QC-Functions: Automatic QC-sample handling and QC-Chart

Interface

Display: Full-color, touch-sensitive, 15” high-resolution LCD screen with virtual keyboard Languages: English, Chinese

Printer: USB interface for label printer or full-size HP/PCL printer

LIMS interface: Ethernet or RS232, Automatic LIMS transfer

Data Export: USB Memory Stick, Import into Excel

Password Protection: Different access levels for Operator, Manager, Service

Diagnostics: Automatic diagnostic functions

Accessories: Barcode Reader, label printer

Utility Requirements

Electrical: 90V to 260 VAC; 47-63Hz; 350W

Ambient Conditions: Temperature: max. 10° to 30°C; extremes not recommended

Dimensions: 54.6 cm (21.5”) deep x 33.7 cm (13.25”) wide x 44.5 cm (17.5”) high

Weight Unit: 24 kg (53 lb.)

Boxed: 28 kg (62 lb.)

Documentation

Title Description PDF
Brochure WAT 70Xi Brochure Download
Brochure WAT-70Xi Marine Fuel Analyzer Download
Press Article Improved Automatic Test for WAT of Crude Download

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